7SIY
cCBL TKB domain in complex with pZAP70 peptide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-13 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979460 |
Spacegroup name | P 6 |
Unit cell lengths | 123.519, 123.519, 56.598 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.660 - 1.480 |
R-factor | 0.2092 |
Rwork | 0.208 |
R-free | 0.22090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ob2 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.691 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | DIMPLE |
Refinement software | PHENIX (1.19-4092_final) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 61.759 | 1.501 |
High resolution limit [Å] | 1.476 | 1.476 |
Rmerge | 8.110 | |
Number of reflections | 78431 | 4096 |
<I/σ(I)> | 7.9 | 0.4 |
Completeness [%] | 94.7 | |
Redundancy | 9.9 | |
CC(1/2) | 1.000 | 0.346 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M Ammonium formate, 20% PEG3350 |