7SGA
[C-S] DNA mismatch in a self-assembling rhombohedral lattice
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-10-24 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.00743 |
Spacegroup name | H 3 |
Unit cell lengths | 108.614, 108.614, 92.586 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 33.190 - 3.150 |
R-factor | 0.2328 |
Rwork | 0.232 |
R-free | 0.24260 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5w6w |
RMSD bond length | 0.007 |
RMSD bond angle | 0.987 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 65.984 | 65.984 | 3.974 |
High resolution limit [Å] | 3.150 | 10.263 | 3.150 |
Number of reflections | 2869 | 204 | 206 |
<I/σ(I)> | 8.8 | 29.2 | 2.2 |
Completeness [%] | 63.7 | ||
Redundancy | 10.7 | ||
CC(1/2) | 1.000 | 1.000 | 0.897 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.8 | 293 | MOPS, Magnesium sulfate |