7SDV
[T:Ag+:mC] Metal-mediated DNA base pair in a self-assembling rhombohedral lattice
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-18 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.0743 |
Spacegroup name | H 3 |
Unit cell lengths | 105.128, 105.128, 91.029 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.190 - 4.190 |
R-factor | 0.241 |
Rwork | 0.237 |
R-free | 0.32170 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 0.939 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | AutoSol |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.469 | 4.328 |
High resolution limit [Å] | 4.001 | 4.001 |
Rpim | 3.354 | |
Number of reflections | 2167 | 197 |
<I/σ(I)> | 5.3 | 0.5 |
Completeness [%] | 88.7 | 69.4 |
Redundancy | 10.7 | |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.8 | 293 | MOPS, Magnesium sulfate, Silver nitrate |