7SDL
[S:Ag+:T] Metal-mediated DNA base pair in a self-assembling rhombohedral lattice
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-10-24 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.65313 |
Spacegroup name | H 3 |
Unit cell lengths | 105.917, 105.917, 93.855 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.800 - 4.370 |
R-factor | 0.2032 |
Rwork | 0.200 |
R-free | 0.26640 |
Structure solution method | SAD |
RMSD bond length | 0.017 |
RMSD bond angle | 1.149 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | AutoSol |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 32.800 | 32.800 | 4.969 |
High resolution limit [Å] | 4.368 | 10.267 | 4.368 |
Number of reflections | 1730 | 192 | 192 |
<I/σ(I)> | 10.6 | 32.6 | |
Completeness [%] | 84.8 | 99 | 50.9 |
Redundancy | 10.3 | 10.2 | 10.7 |
CC(1/2) | 0.994 | 0.992 | 0.197 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.8 | 293 | MOPS, Magnesium sulfate, Silver nitrate |