7S0Z
Structures of TcdB in complex with R-Ras
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-12-11 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 76.308, 112.112, 101.571 |
Unit cell angles | 90.00, 95.89, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 112.110 | 2.390 |
High resolution limit [Å] | 2.340 | 2.340 |
Rmerge | 0.085 | |
Number of reflections | 70923 | 4599 |
<I/σ(I)> | 9.6 | |
Completeness [%] | 98.9 | |
Redundancy | 3.4 | |
CC(1/2) | 0.993 | 0.693 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.2M ammonium acetate, 0.1M sodium citrate tribasic dihydrate, pH 4.8, and 17% PEG 4000 |