7RZ1
Hen egg-white lysozyme with ionic liquid ethanolammonium formate 14.4 mol%
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-05-02 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 1.23980 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 76.650, 76.650, 38.290 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.200 - 2.046 |
Rwork | 0.160 |
R-free | 0.24310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7jmu |
RMSD bond length | 0.010 |
RMSD bond angle | 1.776 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.200 | 2.100 |
High resolution limit [Å] | 2.046 | 2.050 |
Number of reflections | 7613 | 571 |
<I/σ(I)> | 11.3 | 2.8 |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.7 | |
CC(1/2) | 0.981 | 0.852 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | ethanolammonium formate 14.4mol% (ca. 50wt%) in water |