7RYD
Hen egg-white lysozyme with ionic liquid butylammonium nitrate 1 mol%
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-02-06 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.95372 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 27.640, 62.450, 59.780 |
Unit cell angles | 90.00, 90.21, 90.00 |
Refinement procedure
Resolution | 17.090 - 1.180 |
Rwork | 0.199 |
R-free | 0.22994 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7jmu |
RMSD bond length | 0.014 |
RMSD bond angle | 1.893 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.180 | 1.200 |
High resolution limit [Å] | 1.180 | 1.180 |
Number of reflections | 67030 | 3344 |
<I/σ(I)> | 5.4 | 1.1 |
Completeness [%] | 99.8 | 99.6 |
Redundancy | 6.2 | |
CC(1/2) | 0.992 | 0.036 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 8 | 298.15 | butylammonium nitrate 1 mol% (ca. 7wt%) in water |