7RTX
Actophorin grown in microgravity
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 39.810, 45.800, 69.310 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.660 - 1.650 |
R-factor | 0.1902 |
Rwork | 0.188 |
R-free | 0.22330 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ahq |
RMSD bond length | 0.012 |
RMSD bond angle | 1.202 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.660 | 1.709 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.077 | 0.875 |
Number of reflections | 28851 | 1542 |
<I/σ(I)> | 11.63 | |
Completeness [%] | 99.5 | |
Redundancy | 6.1 | |
CC(1/2) | 0.998 | 0.816 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 298 | 10 mg/mL protein, 0.1 M MOPS, 16% Polyethylene glycol (8,000) |