7RI0
Aspergillus fumigatus Enolase Bound to Phosphoenolpyruvate and 2-Phosphoglycerate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-09-30 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.954 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 67.858, 84.154, 84.909 |
Unit cell angles | 90.00, 98.04, 90.00 |
Refinement procedure
Resolution | 42.497 - 2.300 |
R-factor | 0.2103 |
Rwork | 0.208 |
R-free | 0.25500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7rhv |
Data reduction software | XDS (20190315) |
Data scaling software | Aimless (0.5.25) |
Phasing software | PHASER (2.8.2) |
Refinement software | PHENIX (1.16-3549) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.900 | 46.900 | 2.380 |
High resolution limit [Å] | 2.300 | 8.910 | 2.300 |
Rmerge | 0.109 | 0.063 | 0.342 |
Rmeas | 0.118 | 0.069 | 0.368 |
Rpim | 0.044 | 0.026 | 0.136 |
Total number of observations | 302573 | 5243 | 29996 |
Number of reflections | 42138 | 764 | 4090 |
<I/σ(I)> | 13.3 | 23.5 | 4.7 |
Completeness [%] | 99.9 | 99.2 | 99.9 |
Redundancy | 7.2 | 6.9 | 7.3 |
CC(1/2) | 0.995 | 0.996 | 0.965 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 289.15 | 21% PEG 3350, 0.05 M Bis-Tris |