7RED
Holo Hemophilin from A. baumannii
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 105 |
Detector technology | CCD |
Collection date | 2016-07-19 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.9796 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.900, 59.550, 63.740 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.692 - 1.530 |
R-factor | 0.1486 |
Rwork | 0.148 |
R-free | 0.16690 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.692 | 1.585 |
High resolution limit [Å] | 1.530 | 1.530 |
Number of reflections | 29892 | 2914 |
<I/σ(I)> | 31.93 | |
Completeness [%] | 100.0 | |
Redundancy | 14.4 | |
CC(1/2) | 1.000 | 0.979 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.15 | 293 | 100 mM sodium acetate pH 4.15, 3.25 M sodium formate |