7R5P
Strep-tag FtrA-P19 from Rubrivivax gelatinosus in complex with copper and iron
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-02-07 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.980115 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.575, 77.996, 115.225 |
Unit cell angles | 90.00, 95.83, 90.00 |
Refinement procedure
Resolution | 32.240 - 1.680 |
R-factor | 0.181 |
Rwork | 0.179 |
R-free | 0.21100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7r3p |
RMSD bond length | 0.010 |
RMSD bond angle | 1.040 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.000 | 1.860 |
High resolution limit [Å] | 1.680 | 1.680 |
Rmerge | 0.077 | 0.738 |
Number of reflections | 92927 | 4342 |
<I/σ(I)> | 11.4 | |
Completeness [%] | 99.5 | |
Redundancy | 6.4 | |
CC(1/2) | 0.998 | 0.725 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 292 | 25% PEG4K, 0.1 M Tris-HCl, 0.2 M MgCl2 |