7R3S
FtrA/P19 of Rubrivivax gelatinosus in complex with Ni
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-27 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 1.48484 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.280, 79.810, 82.410 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.590 - 1.790 |
R-factor | 0.177 |
Rwork | 0.176 |
R-free | 0.20100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7r3p |
RMSD bond length | 0.010 |
RMSD bond angle | 1.070 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.590 | 1.900 |
High resolution limit [Å] | 1.790 | 1.790 |
Rmerge | 0.078 | |
Number of reflections | 68702 | 10524 |
<I/σ(I)> | 12.2 | |
Completeness [%] | 99.8 | |
Redundancy | 6 | |
CC(1/2) | 0.998 | 0.561 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 292 | 2M AS, 0.1 M Citrate Sodium, 0.02 M NiSO4 |