7R30
Carbon regulatory PII-like protein SbtB from Synechocystis sp. 6803 in complex with ADP and AMP resulting from ADP soak
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-24 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.000 |
Spacegroup name | P 32 |
Unit cell lengths | 63.637, 63.637, 82.207 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.950 - 1.900 |
R-factor | 0.1721 |
Rwork | 0.171 |
R-free | 0.19450 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 5o3p |
RMSD bond length | 0.020 |
RMSD bond angle | 2.074 |
Data reduction software | XDS |
Data scaling software | XDS |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.950 | 2.010 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.058 | 1.537 |
Number of reflections | 29447 | 4769 |
<I/σ(I)> | 20.5 | 1.58 |
Completeness [%] | 100.0 | 100 |
Redundancy | 10.3 | 10.3 |
CC(1/2) | 0.999 | 0.713 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294 | 0.2 M SODIUM ACETATE, 0.1 M HEPES PH 7.5, 20 % (W/V) PEG3000 |