7R0N
KRasG12C in complex with GDP and compound 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-08-05 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 41.351, 59.228, 65.207 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.500 - 1.200 |
R-factor | 0.203 |
Rwork | 0.202 |
R-free | 0.22200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1WXEX |
RMSD bond length | 0.008 |
RMSD bond angle | 1.020 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.8) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.210 | 1.230 |
High resolution limit [Å] | 1.200 | 1.200 |
Rmerge | 0.039 | 0.696 |
Number of reflections | 50779 | 1016 |
<I/σ(I)> | 19.8 | 2.24 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 6.22 | 5.58 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 33% PEG 6000, 0.01 M NaCitrate |