7QXR
Azacoelenterazine-bound Renilla-type luciferase (AncFT)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-05-12 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.284, 87.549, 102.693 |
Unit cell angles | 90.00, 93.46, 90.00 |
Refinement procedure
Resolution | 46.944 - 2.052 |
R-factor | 0.1952 |
Rwork | 0.192 |
R-free | 0.24700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6s97 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.944 | 2.110 |
High resolution limit [Å] | 2.050 | 2.050 |
Number of reflections | 56440 | 4304 |
<I/σ(I)> | 9.8 | |
Completeness [%] | 99.5 | |
Redundancy | 6.9 | |
CC(1/2) | 0.997 | 0.591 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293.15 | magnesium chloride, Bis-tris, PEG 3350 |