7QLJ
Trans structure of rsKiiro Illuminated at 290 K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-01-13 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.91587 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 38.747, 73.524, 78.106 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.053 | 1.039 |
High resolution limit [Å] | 1.020 | 1.020 |
Rmerge | 0.061 | 0.777 |
Number of reflections | 112855 | 5645 |
<I/σ(I)> | 12.8 | 2.2 |
Completeness [%] | 98.9 | |
Redundancy | 6.1 | |
CC(1/2) | 0.999 | 0.593 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 8.4 | 295 | 0.2 M lithium sulfate, 0.1 M Tris-Cl, 25 % PEG 3350 |