7QBD
TC:CD320 in complex with nanobody TC-Nb26
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-03-11 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 102.129, 102.129, 360.998 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.140 - 4.180 |
R-factor | 0.2621 |
Rwork | 0.262 |
R-free | 0.27240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4zrp |
RMSD bond length | 0.038 |
RMSD bond angle | 2.004 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.240 | 4.330 |
High resolution limit [Å] | 4.180 | 4.180 |
Number of reflections | 28382 | 1406 |
<I/σ(I)> | 10.17 | |
Completeness [%] | 95.0 | |
Redundancy | 2 | |
CC(1/2) | 0.999 | 0.851 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 297.15 | 150 mM Ammonium citrate tribasic pH 7.0, 21% w/v PEG 3350 |