7QAB

NMR Solution Structure of mussel adhesive protein Pvfp-5b

Spectrometer

Experimental method: SOLUTION NMR

Spectrometer ID	Spectrometer maker	Spectrometer model	Spectrometer type	Spectrometer field strength
1	Bruker	AVANCE NEO		800
2	Bruker	AVANCE III HD		700

Experiment

experiment id	conditions id	solution id	Experiment type
1	1	2	2D 1H-15N HSQC
10	1	2	3D HNCACB
11	1	2	3D HBHA(CO)NH
12	1	2	3D HBHANH
13	1	2	3D 1H-13C NOESY aliphatic
14	1	2	3D 1H-13C NOESY aromatic
15	1	2	3D 1H-15N NOESY
16	1	2	3D HCCH-TOCSY aliphatic
17	1	1	3D HCCH-TOCSY aromatic
2	1	2	2D 1H-13C HSQC
3	1	2	2D HBCBCGCDHD
4	1	2	2D HBCBCGCDCEHE
5	1	1	3D HNCO
6	1	1	3D HNCA
8	1	1	3D HN(CO)CA
9	1	2	3D HN(COCA)CB

NMR Sample

conditions id	NMR sample pH	NMR sample pressure	NMR sample temperature
1	4.5	1	298
2	4.5	1	298

Conformers

Conformers Calculated Total Number	20
Conformers Submitted Total Number	20