7PXT
Structure of an LPMO, collected from serial synchrotron crystallography data.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-15 |
Detector | PSI JUNGFRAU 4M |
Wavelength(s) | 0.98 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 125.420, 125.420, 125.420 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.690 - 2.400 |
R-factor | 0.19 |
Rwork | 0.187 |
R-free | 0.24760 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 5ach |
RMSD bond length | 0.007 |
RMSD bond angle | 1.464 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.690 | 2.460 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmeas | 0.293 | 0.910 |
Number of reflections | 21952 | 1698 |
<I/σ(I)> | 7.21 | 3.37 |
Completeness [%] | 88.0 | 89.7 |
Redundancy | 3.51 | 3.59 |
CC(1/2) | 0.619 | 0.664 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4 | 298 | 4.1 M NaCl, 0.1 M citric acid pH 4.0 The crystals were equilibrated in a drop of 3.5 M NaCl, 0.1 M citric acid pH 5.5 |