Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 80 |
| Detector technology | PIXEL |
| Collection date | 2019-02-13 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97918 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 79.407, 150.429, 107.370 |
| Unit cell angles | 90.00, 98.85, 90.00 |
Refinement procedure
| Resolution | 75.328 - 2.750 |
| R-factor | 0.20371 |
| Rwork | 0.201 |
| R-free | 0.25875 |
| Structure solution method | SAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.460 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 75.330 | 2.821 |
| High resolution limit [Å] | 2.750 | 2.750 |
| Number of reflections | 61491 | 4301 |
| <I/σ(I)> | 8.3 | |
| Completeness [%] | 95.1 | |
| Redundancy | 4.4 | |
| CC(1/2) | 0.976 | 0.586 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 294 | 20% PEG 10.000 and 0.1 M Na-Hepes pH7.5 |
