7PUQ
CARM1 in complex with EML982
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-11-08 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 75.128, 98.694, 207.778 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.010 - 2.090 |
R-factor | 0.1829 |
Rwork | 0.181 |
R-free | 0.21740 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5ih3 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.010 | 2.120 |
High resolution limit [Å] | 2.090 | 2.090 |
Rmerge | 0.085 | 1.330 |
Rmeas | 0.089 | 1.387 |
Rpim | 0.024 | 0.386 |
Number of reflections | 92014 | 4053 |
<I/σ(I)> | 17.8 | 1.8 |
Completeness [%] | 99.5 | 90.2 |
Redundancy | 13.4 | 12 |
CC(1/2) | 1.000 | 0.831 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 12% PEG 3350, 0.1 M NaCl, 0.1 M TrisHCl pH8.5 |