7PUJ
Crystal structure of Endoglycosidase E GH18 domain from Enterococcus faecalis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-09-08 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 0.9792 |
Spacegroup name | P 65 |
Unit cell lengths | 112.150, 112.150, 64.620 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 38.820 - 1.752 |
R-factor | 0.1879 |
Rwork | 0.186 |
R-free | 0.22040 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6mdv |
RMSD bond length | 0.024 |
RMSD bond angle | 0.787 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.820 | 1.815 |
High resolution limit [Å] | 1.752 | 1.752 |
Rmerge | 0.060 | 0.908 |
Rmeas | 0.062 | 0.946 |
Number of reflections | 46562 | 4569 |
<I/σ(I)> | 34.02 | 2.73 |
Completeness [%] | 99.9 | 99.05 |
Redundancy | 19.1 | 13 |
CC(1/2) | 1.000 | 0.839 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 20 mM zinc chloride, 20% w/v PEG 3350 |