7PSO
Cereblon isoform 4 from Magnetospirillum gryphiswaldense in complex with Avadomide (CC-122)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-09 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.562, 60.162, 88.406 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.240 - 1.520 |
R-factor | 0.1861 |
Rwork | 0.184 |
R-free | 0.21690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4v2y |
RMSD bond length | 0.012 |
RMSD bond angle | 1.862 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0266) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.240 | 1.610 |
High resolution limit [Å] | 1.520 | 1.520 |
Rmerge | 0.066 | 1.337 |
Rmeas | 0.069 | 1.392 |
Number of reflections | 47297 | 7506 |
<I/σ(I)> | 18.96 | |
Completeness [%] | 99.9 | 99.4 |
Redundancy | 12 | 12 |
CC(1/2) | 0.999 | 0.783 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.5 M (NH4)H2PO4 |