7PRK
Factor XII Fibronectin type II (FXII FnII) domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-09-17 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.2821 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 45.820, 45.820, 53.500 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.800 - 1.640 |
R-factor | 0.1713 |
Rwork | 0.170 |
R-free | 0.20420 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | FXII FnII from unpublished structure |
RMSD bond length | 0.011 |
RMSD bond angle | 1.555 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.800 | 1.670 |
High resolution limit [Å] | 1.640 | 1.640 |
Number of reflections | 7469 | 351 |
<I/σ(I)> | 26.6 | |
Completeness [%] | 100.0 | |
Redundancy | 10.2 | |
CC(1/2) | 0.999 | 0.983 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 292.15 | 0.1 M Sodium Cacodylate, 25 % (w/v) PEG 4000 |