7PNI
X-ray structure of the adduct formed upon reaction of Pt(II) complex 2c with ribonuclease A
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 11.2C |
Synchrotron site | ELETTRA |
Beamline | 11.2C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-03-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.96 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 100.140, 31.790, 73.740 |
Unit cell angles | 90.00, 90.35, 90.00 |
Refinement procedure
Resolution | 28.040 - 2.130 |
Rwork | 0.192 |
R-free | 0.27500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jvt |
RMSD bond length | 0.010 |
RMSD bond angle | 2.195 |
Data reduction software | MOSFLM |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.040 | 2.170 |
High resolution limit [Å] | 2.130 | 2.130 |
Rmerge | 0.078 | 0.643 |
Rmeas | 0.086 | 0.721 |
Rpim | 0.034 | 0.318 |
Number of reflections | 13153 | 649 |
<I/σ(I)> | 14.5 | 2.3 |
Completeness [%] | 99.0 | 97.3 |
Redundancy | 6.2 | 4.9 |
CC(1/2) | 0.998 | 0.898 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.1 | 293 | 22% PEG4K 10 mM sodium citrate pH 5.1 |