7PNH

X-ray structure of the adduct formed upon reaction of Pt(II) complex 2c with lysozyme

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 11.2C
Synchrotron site	ELETTRA
Beamline	11.2C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-03-04
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.96
Spacegroup name	P 43 21 2
Unit cell lengths	77.200, 77.200, 38.530
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	34.520 - 1.220
Rwork	0.133
R-free	0.17410
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	193l
RMSD bond length	0.020
RMSD bond angle	2.273
Data reduction software	MOSFLM
Data scaling software	autoPROC
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	34.520	1.240
High resolution limit [Å]	1.220	1.220
Rmerge	0.056	1.531
Rmeas	0.057	1.564
Rpim	0.012	0.315
Number of reflections	35283	1737
<I/σ(I)>	24.5	2.2
Completeness [%]	100.0	100
Redundancy	23.2	24.3
CC(1/2)	1.000	0.861

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4	293	20% ethylene glycol 0.1 M sodium acetate buffer pH 4.0 0.6 M sodium nitrate