7PL7
Crystal structure of yeast Otu2 OTU domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-10-16 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.979 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 44.669, 60.055, 148.349 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.772 - 2.600 |
R-factor | 0.2271 |
Rwork | 0.225 |
R-free | 0.26430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4bou |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.772 | 42.772 | 2.750 |
High resolution limit [Å] | 2.590 | 7.660 | 2.590 |
Rmerge | 0.132 | 0.043 | 1.002 |
Rmeas | 0.142 | 0.047 | 1.080 |
Total number of observations | 84923 | ||
Number of reflections | 11976 | 469 | 1925 |
<I/σ(I)> | 13.95 | 39.32 | 2.35 |
Completeness [%] | 99.8 | 99.4 | 98.5 |
Redundancy | 7.091 | 6.746 | 7.197 |
CC(1/2) | 0.998 | 0.999 | 0.898 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 0.2 M KSCN 0.1 M BisTris propane pH 6.5 20% PEG 3350 20% glycerol |