7PJK
Cereblon isoform 4 from Magnetospirillum gryphiswaldense in complex with a benzotriazole analog of thalidomide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-09 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.779, 59.435, 88.189 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.440 - 1.990 |
R-factor | 0.2107 |
Rwork | 0.208 |
R-free | 0.25440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4v2y |
RMSD bond length | 0.003 |
RMSD bond angle | 1.305 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0266) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.440 | 2.110 |
High resolution limit [Å] | 1.990 | 1.990 |
Rmerge | 0.095 | 1.810 |
Number of reflections | 21052 | 3305 |
<I/σ(I)> | 14.9 | 1.25 |
Completeness [%] | 99.7 | 98.3 |
Redundancy | 12.8 | 13 |
CC(1/2) | 0.999 | 0.583 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.4 M (NH4)2HPO4 |