7PAZ
REDUCED MUTANT P80I PSEUDOAZURIN FROM A. FAECALIS
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1994-05 |
Detector | RIGAKU RAXIS |
Spacegroup name | P 65 |
Unit cell lengths | 50.790, 50.790, 98.250 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 26.000 - 2.000 |
R-factor | 0.2 * |
RMSD bond length | 0.004 * |
RMSD bond angle | 0.018 |
Data reduction software | R-AXIS |
Data scaling software | R-AXIS |
Refinement software | SHELXL |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.000 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.060 * | 0.110 |
Number of reflections | 9327 | |
<I/σ(I)> | 10 | 3 |
Completeness [%] | 96.0 * | 90 * |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.8 * | 50MM SODIUM PHOSPHATE WITH 75%, pH 7.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | 20 (mg/ml) | |
2 | 1 | 1 | phosphate | 20 (mM) | |
3 | 1 | 1 | ammonium sulfate | 42 (%sat) |