7P9Z
Crystal structure of a trapped Pab-AGOG/double-standed DNA covalent intermediate (DNA containing adenine opposite to lesion)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-02 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.98011 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 61.848, 68.775, 68.424 |
Unit cell angles | 90.00, 90.35, 90.00 |
Refinement procedure
Resolution | 45.990 - 1.330 |
R-factor | 0.1746 |
Rwork | 0.174 |
R-free | 0.18650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7oy7 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | PHENIX (1.19_4092) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.420 | 1.350 |
High resolution limit [Å] | 1.330 | 1.330 |
Rmerge | 0.044 | 0.498 |
Number of reflections | 66075 | 3311 |
<I/σ(I)> | 17.2 | 2.2 |
Completeness [%] | 99.5 | |
Redundancy | 6.5 | |
CC(1/2) | 0.999 | 0.924 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | MgCl2, Na acetate pH 5.0, MPD |