7P73
The PDZ domain of SYNJ2BP complexed with the PDZ-binding motif of HTLV1-TAX1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-02-14 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.98 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 60.450, 63.990, 146.950 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.000 | 1.900 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmeas | 0.142 | 2.290 |
Number of reflections | 48765 | 3522 |
<I/σ(I)> | 15.18 | 1.75 |
Completeness [%] | 98.3 | |
Redundancy | 13.6 | |
CC(1/2) | 0.999 | 0.593 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 120mM Monosaccharides, 100mM Buffer System 3 pH 8.5, 50 % Precipitant Mix 2 (F10 Morpheus) |