7P4T
Tetrameric structure of murine SapA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-08 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 65 |
Unit cell lengths | 48.489, 48.489, 314.359 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 52.400 - 3.170 |
Rwork | 0.272 |
R-free | 0.30400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ddj |
RMSD bond length | 0.003 |
RMSD bond angle | 0.774 |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.400 | 3.420 |
High resolution limit [Å] | 3.170 | 3.170 |
Rmerge | 0.178 | |
Rpim | 0.059 | 0.585 |
Number of reflections | 5576 | 372 |
<I/σ(I)> | 5.5 | 1.1 |
Completeness [%] | 91.8 | |
Redundancy | 10.1 | |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 23.25% (w/v) PEG 3350, 0.1 M Bis-Tris pH 5.6 |