7P3A
N-terminal domain of CGI-99
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-03-14 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.0084 |
Spacegroup name | P 61 |
Unit cell lengths | 91.714, 91.714, 52.942 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.860 - 2.000 |
R-factor | 0.1979 |
Rwork | 0.197 |
R-free | 0.22420 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.105 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX (1.16_3549) |
Refinement software | PHENIX (1.16_3549) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.860 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.142 | 1.530 |
Rpim | 0.032 | 0.354 |
Number of reflections | 17246 | 3450 |
<I/σ(I)> | 18.6 | 1.9 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 20.2 | 19.3 |
CC(1/2) | 0.999 | 0.740 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 100 mM HEPES pH 7.5, 200 mM magnesium chloride, 20% isopropanol |