7OXW
CrabP2 mutant R30DK31D
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-21 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 45.300, 92.290, 98.760 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.145 - 1.160 |
Rwork | 0.162 |
R-free | 0.17370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2frs |
RMSD bond length | 0.013 |
RMSD bond angle | 1.720 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.150 | 1.180 |
High resolution limit [Å] | 1.160 | 1.160 |
Number of reflections | 71395 | 3221 |
<I/σ(I)> | 19.4 | 2.5 |
Completeness [%] | 99.4 | 91.8 |
Redundancy | 6.4 | 2.8 |
CC(1/2) | 0.999 | 0.946 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 100 mM Sodium acetate pH 4.5 and 2.0 M ammonium sulfate |