7OWL
Odinarchaeota Adenylate kinase (OdinAK) in complex with CTP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-06-03 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9800 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 76.486, 77.631, 216.881 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.010 - 2.900 |
R-factor | 0.1947 |
Rwork | 0.192 |
R-free | 0.25460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7owe |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.010 | 3.080 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.315 | 1.732 |
Rpim | 0.163 | 0.904 |
Number of reflections | 29184 | 2878 |
<I/σ(I)> | 5.5 | 2.1 |
Completeness [%] | 99.3 | 100 |
Redundancy | 8.9 | |
CC(1/2) | 0.986 | 0.628 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | Protein buffer: 0.030 M MOPS, 0.050 M NaCl pH 7.0. Crystallization: Bis-Tris Propane pH 7.0, 0.1 M, PEG 3350 12-18% Odin 0.678 milliM, CTP 6.37 milliM |