7OWK
Odinarchaeota Adenylate kinase (OdinAK) in complex with dTTP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-06-02 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9800 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 76.824, 77.203, 214.745 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.567 - 3.100 |
R-factor | 0.208 |
Rwork | 0.206 |
R-free | 0.26100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7owe |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.570 | 3.210 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.356 | 3.017 |
Number of reflections | 23925 | 2363 |
<I/σ(I)> | 9.1 | 2.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 13.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | Protein: 0.030 M MOPS, 0.050 M NaCl pH 7.0. Precipitant: Bis-Tris Propane pH 7.0, 0.1 M, PEG 3350 15-18% Odin 0.732 milliM, dTTP 5.8 milliM |