7OQN
Human OMPD-domain of UMPS in complex with substrate OMP at 1.10 Angstroms resolution, 30 minutes soaking
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-08 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.827 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.059, 61.891, 70.097 |
Unit cell angles | 90.00, 113.12, 90.00 |
Refinement procedure
Resolution | 42.540 - 1.100 |
R-factor | 0.1328 |
Rwork | 0.132 |
R-free | 0.14960 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6zwy |
RMSD bond length | 0.008 |
RMSD bond angle | 1.499 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.540 | 42.540 | 1.130 |
High resolution limit [Å] | 1.100 | 4.920 | 1.100 |
Rmerge | 0.042 | 0.014 | 0.721 |
Rmeas | 0.050 | 0.017 | 0.860 |
Total number of observations | 763641 | ||
Number of reflections | 220244 | 2488 | 16213 |
<I/σ(I)> | 15.36 | 75.52 | 1.74 |
Completeness [%] | 98.7 | 95.3 | 98.4 |
Redundancy | 3.467 | 3.328 | 3.403 |
CC(1/2) | 1.000 | 0.999 | 0.745 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.8 | 293.15 | Ammonium sulfate, Tris/HCl, Glutathion, Glycerol |