7OQM
Human OMPD-domain of UMPS in complex with substrate OMP at 1.05 Angstroms resolution, 20 minutes soaking
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-08 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.827 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 69.964, 61.882, 70.052 |
Unit cell angles | 90.00, 113.09, 90.00 |
Refinement procedure
Resolution | 42.510 - 1.050 |
R-factor | 0.1216 |
Rwork | 0.121 |
R-free | 0.13360 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6zwy |
RMSD bond length | 0.007 |
RMSD bond angle | 1.468 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.510 | 42.510 | 1.080 |
High resolution limit [Å] | 1.050 | 4.700 | 1.050 |
Rmerge | 0.050 | 0.023 | 0.800 |
Rmeas | 0.059 | 0.027 | 0.963 |
Total number of observations | 868228 | ||
Number of reflections | 248705 | 2836 | 17591 |
<I/σ(I)> | 12.35 | 46.64 | 1.7 |
Completeness [%] | 97.2 | 94.9 | 93.3 |
Redundancy | 3.491 | 3.416 | 3.19 |
CC(1/2) | 0.999 | 0.999 | 0.661 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.8 | 293.15 | Ammonium sulfate, Tris/HCl, Glutathion, Glycerol |