7OOI
Anti-EphA1 JD1 VH domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-09-15 |
Detector | RAYONIX MX-300 |
Wavelength(s) | 0.979490 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 60.210, 60.210, 168.071 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.580 - 2.280 |
Rwork | 0.269 |
R-free | 0.29700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3b9v |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (v1.14) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 42.580 | 6.380 | 2.280 |
High resolution limit [Å] | 2.150 | 6.380 | 2.150 |
Rmerge | 0.260 | 0.068 | 2.284 |
Rmeas | 0.270 | 0.071 | 2.377 |
Number of reflections | 17674 | 785 | 2751 |
<I/σ(I)> | 10.62 | 27.09 | 2.01 |
Completeness [%] | 99.9 | 99.7 | 99.7 |
Redundancy | 13.552 | 12.005 | 12.716 |
CC(1/2) | 0.997 | 0.999 | 0.724 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | 0.2 M ammonium sulphate, 10% glycerol, 0.1 M phosphate citrate (pH 4.2) and 20% (w/v) polyethyleneglycol (PEG) 300 |