7OKS
X-ray structure of soluble EPCR in P212121 space group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-01-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97926 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.437, 94.019, 124.595 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.320 - 1.950 |
R-factor | 0.201 |
Rwork | 0.199 |
R-free | 0.23930 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1lqv |
RMSD bond length | 0.009 |
RMSD bond angle | 1.077 |
Data reduction software | XDS (BUILT=20190315) |
Data scaling software | Aimless (0.7.4) |
Phasing software | PHASER (2.8.3) |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.530 | 2.000 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.089 | 1.081 |
Rmeas | 0.097 | |
Rpim | 0.038 | 0.447 |
Number of reflections | 67837 | 4494 |
<I/σ(I)> | 10.1 | 1.6 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 6.5 | 6.8 |
CC(1/2) | 0.998 | 0.867 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | 2.8 M sodium acetate pH 8.0, 0.1 M Tris pH 7.0 |