7OIY
Crystal structure of the ZUFSP family member Mug105
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-01-28 |
Detector | DECTRIS EIGER R 4M |
Wavelength(s) | 0.967700 |
Spacegroup name | P 41 |
Unit cell lengths | 88.235, 88.235, 111.011 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.460 - 2.050 |
R-factor | 0.1738 |
Rwork | 0.173 |
R-free | 0.20390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ei1 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.500 |
Data reduction software | XDS (20180126) |
Data scaling software | XDS (20180126) |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.1_4122) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.460 | 2.124 |
High resolution limit [Å] | 2.050 | 2.050 |
Number of reflections | 53097 | 5246 |
<I/σ(I)> | 10.35 | |
Completeness [%] | 99.8 | |
Redundancy | 6 | |
CC(1/2) | 0.998 | 0.441 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.8 M sodium acetate pH 7.0; 0.1 M BIS-TRIS propane pH 7.0 |