7OHL
SaFtsZ complexed with GDP, BeF3- and Mn2+
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 72.020, 51.490, 88.020 |
Unit cell angles | 90.00, 110.82, 90.00 |
Refinement procedure
Resolution | 41.140 - 1.750 |
R-factor | 0.1717 |
Rwork | 0.170 |
R-free | 0.21130 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6rvn |
RMSD bond length | 0.030 |
RMSD bond angle | 3.237 |
Data reduction software | XDS (1.18.2_3874) |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.140 | 1.850 |
High resolution limit [Å] | 1.750 | 1.750 |
Number of reflections | 30098 | 2991 |
<I/σ(I)> | 8.15 | |
Completeness [%] | 98.4 | |
Redundancy | 4.7 | |
CC(1/2) | 0.997 | 0.334 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Tris-HCl pH 8.8, 25% PEG 5000 MME |