7OEC
Crystal structure of an intein from a hyperthermophile
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-24 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 70.820, 70.820, 70.660 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.410 - 1.480 |
R-factor | 0.1555 |
Rwork | 0.154 |
R-free | 0.18680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6rpq |
RMSD bond length | 0.017 |
RMSD bond angle | 1.483 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.410 | 1.533 |
High resolution limit [Å] | 1.480 | 1.480 |
Number of reflections | 30560 | 2977 |
<I/σ(I)> | 16.35 | 4.22 |
Completeness [%] | 99.9 | 99.97 |
Redundancy | 25.4 | |
CC(1/2) | 0.998 | 0.445 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 100 mM MES pH 6, 15 % (W/v) PEG 550 MME, 30 mM zinc sulfate |