7OC9

Structure of Bdellovibrio bacteriovorus Bd0675

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-12-01
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9119
Spacegroup name	C 2 2 21
Unit cell lengths	53.490, 69.670, 85.850
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.428 - 1.500
R-factor	0.1982
Rwork	0.197
R-free	0.21290
Structure solution method	SAD
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX (1.15.2_3472)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.430	1.554
High resolution limit [Å]	1.500	1.500
Rmerge	0.042	1.887
Number of reflections	25800	2533
<I/σ(I)>	24.27
Completeness [%]	99.0
Redundancy	13.1
CC(1/2)	0.999	0.638

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	291	47% v/v MPD 2% t-Butanol