7OC1
Structure of Pseudomonas aeruginosa FabF mutant C164Q in complex with Platensimycin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.918399 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 84.024, 137.199, 65.692 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 68.690 - 1.800 |
R-factor | 0.15882 |
Rwork | 0.157 |
R-free | 0.18773 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4jb6 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.492 |
Data reduction software | xia2 |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 68.690 | 1.850 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.102 | 0.301 |
Rmeas | 0.118 | 0.352 |
Rpim | 0.045 | 0.135 |
Number of reflections | 71222 | 3493 |
<I/σ(I)> | 11.05 | 4.98 |
Completeness [%] | 100.0 | 98.6 |
Redundancy | 6.7 | 6.7 |
CC(1/2) | 0.995 | 0.952 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.24M NH4HCO2 and 31.2% PEG3350 |