7OBP

Crystal structure of the human NCOA7-AS TLDc domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE MASSIF-1
Synchrotron site	ESRF
Beamline	MASSIF-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-03-12
Detector	DECTRIS PILATUS3 2M
Wavelength(s)	0.965
Spacegroup name	P 21 21 21
Unit cell lengths	68.410, 107.060, 146.440
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.290 - 1.800
R-factor	0.1774
Rwork	0.177
R-free	0.22120
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4acj
RMSD bond length	0.005
RMSD bond angle	0.786
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX (1.19_4092)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	45.290	1.860
High resolution limit [Å]	1.800	1.800
Rmeas	0.147	1.140
Number of reflections	100055	9863
<I/σ(I)>	10.1
Completeness [%]	99.7
Redundancy	5.2
CC(1/2)	0.997	0.580

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	4.5	291	0.1 M sodium acetate pH4.5, 30% PEG 300