7OB0
Structure of RsLOV d2 variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | BRUKER IMUS MICROFOCUS |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2020-11-27 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.057, 77.168, 155.002 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.930 - 1.900 |
R-factor | 0.1776 |
Rwork | 0.176 |
R-free | 0.21810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4hia |
RMSD bond length | 0.006 |
RMSD bond angle | 0.918 |
Data reduction software | XDS |
Data scaling software | pointless (1.12.2) |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX (1.19_4092) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.010 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmeas | 0.057 | 0.254 |
Number of reflections | 55587 | 8900 |
<I/σ(I)> | 17.67 | 5.53 |
Completeness [%] | 99.6 | |
Redundancy | 3.93 | |
CC(1/2) | 0.998 | 0.961 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 293 | 0.1 M Imidazole pH 8.0, 22 %(w/v) PEG 1000, 0,2 M Calcium acetate |