Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-07-22 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9762 |
| Spacegroup name | P 31 |
| Unit cell lengths | 108.420, 108.420, 165.538 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 93.895 - 2.340 |
| Rwork | 0.192 |
| R-free | 0.22750 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6zbp |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.611 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 94.000 | 2.400 |
| High resolution limit [Å] | 2.340 | 2.340 |
| Rpim | 0.051 | 0.700 |
| Number of reflections | 91842 | 4643 |
| <I/σ(I)> | 9.9 | 0.8 |
| Completeness [%] | 100.0 | 99.6 |
| Redundancy | 10.1 | 7 |
| CC(1/2) | 1.000 | 0.500 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M SPG, pH 8, 25 % Peg 1500, |
