Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-09-16 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9762 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 105.683, 105.683, 112.539 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 62.254 - 1.901 |
| Rwork | 0.180 |
| R-free | 0.20400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6zbp |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.528 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 62.254 | 1.950 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rpim | 0.025 | |
| Number of reflections | 50645 | 3478 |
| <I/σ(I)> | 14.4 | 0.7 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 25.4 | 22.1 |
| CC(1/2) | 0.990 | 0.940 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.0 M Lithium chloride, 0.1 M Citrate pH 4, 20 % Peg 6000 |
