7O6V
Crystal structure of the VEL1 VEL polymerising domain (R643A K645D I664D mutant)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-10-07 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979500 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.066, 58.053, 119.991 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.040 - 2.500 |
R-factor | 0.21492 |
Rwork | 0.214 |
R-free | 0.24070 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.157 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | CRANK2 |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.040 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 13183 | 1481 |
<I/σ(I)> | 9.6 | |
Completeness [%] | 100.0 | |
Redundancy | 20 | |
CC(1/2) | 0.990 | 0.840 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 291 | 20% PEG 3350, 2M Sodium malonate pH7 |